Download e-book for iPad: Microwave Assisted Organic Synthesis by Jason P. Tierney, Pelle Lidstrom

By Jason P. Tierney, Pelle Lidstrom

ISBN-10: 0849323711

ISBN-13: 9780849323713

Microwave Assisted natural Chemistry demonstrates the less than mendacity ideas of microwave dielectric heating and, by means of connection with a number natural response kinds, its powerful use in artificial natural chemistry. the hot creation of in particular designed and developed microwave apparatus, countering security, and reproducibility matters has ended in common use of microwaves in artificial natural chemistry. Microwave assisted synthesis is now validated in lots of business and educational laboratories giving entry to the radical chemistry that may be performed in a number of natural response varieties. Case reports, drawn from the pharmaceutical undefined, illustrate the impression microwave assisted natural synthesis may have on chemical learn.

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Example text

Stille couplings Lately, a number of papers have dealt with microwave-assisted reactions on palladiumdoped Al2 O3 . Villemin reported on Stille, Suzuki, Heck and Trost–Tsuji reactions where potassium fluoride on alumina was used as the base26 . The reactions were carried out without solvent or stabilising phosphine ligands in single-mode reactors. The Stille reactions were noteworthy as the toxic organotin residue remained adsorbed on the solid support, thus allowing a simplified work-up procedure for the otherwise unpleasant, and toxic, stannous by-products.

5) The boiling phenomenon is a kinetic as well as a thermodynamic process and therefore solvents heated under microwave conditions often boil at elevated temperatures even though they remain contained under 1 atm pressure. The precise elevation of this nucleation-limited boiling point depends on the power input, the occurrence of effective stirring and the limitation of the number of nucleation sites, for example, by having smooth surfaces and no boiling chips. This effect can be enhanced by allowing the pressure to rise above atmospheric level.

Ceram. Soc. , 1989, 68, 1601. 5. , Dielectric Materials and Applications, MIT Press, Cambridge, MA, 1954. 6. , Laberge, L. ,1986, 27, 279. 7. N. , 1986, 28, 4945. 8. P. , Application of microwave dielectric loss heating effects for the rapid and convenient synthesis of organometallic compounds, J. Organomet. , 1989, 368, C43. cls 22 QC: FCH/FFX December 24, 2004 T1: FCH 9:3 MICROWAVE ASSISTED ORGANIC SYNTHESIS 9. P. , Applications of microwave dielectric heating effects to synthetic problems in chemistry, Chem.

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Microwave Assisted Organic Synthesis by Jason P. Tierney, Pelle Lidstrom

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